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    NS3CNPD-3MPL2 Catalyst for 3-Cyanopyridine production from 3-Picoline

    Catalyst for 3-Cyanopyridine production from 3-Picoline successfully developed by Changzhou NEW SOLAR Catalysts Co., Ltd., and started production and sales in 2015. The performance of the product has been evaluated in several batches in the fixed bed pilot-sacle plant study simulating industrial conditions. The catalyst conversion rate is high, the weight yield is good, the product performance is stable, the industrial application life is more than 9 years, and it is still in operation.

    Product Name

    Catalyst for 3-Cyanopyridine production from 3-Picoline

    Product Type NSMA-BSL-BZL2
    Chemical Composition Mixed metal oxides loaded on inert carriers
    Physical Properties

    Type

    NS3CNPD-3MPL2

    Appearance

    Sphere

    Carrier size5±0.5mm

    Bulk density

    0.92±0.1kg/L

    Performance Index

    Oxidation Yield

    grams of 3-cyanopyridine

    produced per 100 grams of 100% pure 3-picoline in the gas phase at the reactor outlet)

    98%-102wt%

    3-methylpyridine conversion

    100% (beginning)99% (ending)

    Hot spot temperature

    370-420℃ (beginning)370-390℃ (normal)

    Catalyst Bed Pressure Drop0.25-0.35kpa
    Catalyst Life ≧3 years

    Commercial Plant Operation Conditions

    3-picoline load per tube

    150g/h normal

    Air flow per tube

    1860NL/h  2400g/h

    Air/3-Cyanopyridine weight ratio:16.0g/g normal Salt temperature

    47g/NCM(normal)、53.8 g/NCM(max)

    Salt Temperature

    345-355℃ (beginning)

    Features

    This type of catalyst is a new generation of catalysts developed in benzene process maleic anhydride catalyst series, which was successfully developed in 2020. Compared with the previous generation of catalysts, the product performance is better and the oxidation yield is high r. At present, most of the newly replaced plants use this type of catalyst.Provide matched catalyst loading and start-up technical services

    Development History

    2013

    Start R&D work

    2013

    R&D succeeded, started production and sales.

    Application Case

    In 2015, a 3-cyanopyridine plant was used for the first time in Shandong, and has been in continuous use for more than 9 years by 2024, with stable performance.

    In 2018, a new 3-cyanopyridine plant in Shandong was used for the first time and has been in continuous use for more than 6 years by 2024, with stable performance

    More new 3-cyanopyridine devices are under negotiation and waiting for the start of the project。